Determination of 16 phthalate metabolites in urine using automated sample preparation and on-line preconcentration/high-performance liquid chromatography/tandem mass spectrometry

Kato, K., Silva, M.J., Needham, L.L., Calafat, A.M.(*)

Div. Lab. Sci., Natl. Cent. Environ. Health, Cent. Dis. Control Prevention, 4770 Buford Hwy, Mailstop F17, Atlanta, GA 30341, USA

REF: Anal. Chem. 77(9) 2005 2985-2991

MS: Finnigan TSQ Quantum, ESP, neg., CAD, SRM.

Keywords: Electrospray/MS/MS, phthalates; CAD; Urine; Isotope dilution; Online SPE-LC/MS; Phthalate esters;

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Determination of tetracycline residues in shrimp and whole milk using liquid chromatography with ultraviolet detection and residue confirmation by mass spectrometry

Andersen, W.C.(*), Roybal, J.E., Gonzales, S.A., Turnipseed, S.B., Pfenning, A.P., Kuck, L.R.

Animal Drugs Res. Cent., US FDA, PO Box 25087, Denver, CO 80225-0087, USA

REF: Anal. Chim. Acta 529(1/2) 2005 145-150

MS: Finnigan TSQ Quantum, ESP, pos., CAD, SRM.

Keywords: Electrospray/MS/MS, antibiotics; CAD; Tetracyclines; Shrimp; Milk; Food; Tetracycline; Oxytetracycline; Chlortetracycline;

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Rapid and decisive determination of Cr6+ using electrospray ionization mass spectrometry

Minakata, K.(*1), Suzuki, M.(2), Suzuki, O.(1)

(1) Dept. Legal Med., (2) Res. Equipment Cent., Hamamatsu Univ. Sch. Med., 1-20-1 Handayama, Hamamatsu 431-3192, Japan

REF: Anal. Chim. Acta 539(1/2) 2005 141-143

MS: Finnigan TSQ 7000, ESP, pos.

Keywords: Electrospray, chromium; Environmental; Chromium complex; Diethyldithiocarbamate; Plasma; Urine; Water;

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Metabolism of aromatic hydrocarbons by the filamentous fungus Cyclothyrium sp.

da Silva, M.(*1), Esposito, E.(2), Moody, J.D.(3), Canhos, V.P.(1), Cerniglia, C.E.(3)

I(1) Dept. Food Sci., Sch. Food Eng., State Univ. Campinas, 13083-970 Campinas, (2) Dept. Environ. Sci., Univ. Mogi das Cruzes, 08780-911 Mogi das Cruzes, Sao Paulo, Brazil, (3) Div. Microbiol., Natl. Cent. Toxicol. Res. US FDA, Jefferson, AR 72079, USA

REF: Chemosphere 57(8) 2004 943-952

MS: Finnigan TSQ 7000, ESP, neg.

Keywords: Electrospray, PAHs; Environmental; Cyclothyrium; Biphenyl; Naphthalene; Anthracene; Phenanthrene; Pyrene; Benzo[a]pyrene; PAHs, metabolism; Microbial degradation;

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Hexabromocyclododecane in marine species from the Western Scheldt estuary: diastereoisomer- and enantiomer-specific accumulation

Janak, K.(*1), Covaci, A.(2), Voorspoels, S.(2), Becher, G.(1)

(1) Div. Environ. Med., Norwegian Inst. Public Health, PO Box 4404, Nydalen, 0403 Oslo, Norway, (2) Toxicol. Cent., Univ. Antwerp, Universiteitsplein 1, 2610 Wilrijk, Belgium

REF: Environ. Sci. Technol. 39(7) 2005 1987-1994

MS: Finnigan TSQ Quantum, ESP, neg., CAD, MRM.

Keywords: Electrospray/MS/MS, hexabromocyclododecane; CAD; Flame retardants; Environmental; Isomer distinction; Enantiomers; Diastereoisomers; Fish; Tissue;

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The structures of five new antifungal and hemolytic amphidinol analogues from Amphidinium carterae collected in New Zealand

Echigoya, R.(1), Rhodes, L.(2), Oshima, Y.(1), Satake, M.(*1)

(1) Grad. Sch. Agric. Sci., Tohoku Univ., 1-1 Tsutsumidori-Amamiya, Aoba-ku, Sendai 981-8555, Japan, (2) Cawthron Inst., 98 Halifax St., PB 2, Nelson, New Zealand

REF: Harmful Algae 4(2) 2005 383-389

MS: Finnigan TSQ 700, ESP, pos., neg.

Keywords: Electrospray, amphidinols; Amphidinium carterae; Algae; Fungicides; Haemolytic activity;

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Analysis of flame retardant additives in polymer fractions of waste of electric and electronic equipment (WEEE) by means of HPLC-UV/MS and GPC-HPLC-UV

Schlummer, M.(*1), Brandl, F.(1), Maurer, A.(1), van Eldik, R.(*2)

(1) Dept. Product Safety Anal., Fraunhofer-Inst. Process Eng. Packaging, Giggenhauser Str. 35, 85354 Freising, (2) Inst. Inorg. Chem., Univ. Erlangen-Nurnberg, Egerlandstr. 1, 91058 Erlangen, Germany

REF: J. Chromatogr. A 1064(1) 2005 39-51

MS: Finnigan TSQ 7000, APCI, neg.

Keywords: APCI, flame retardants; Polybrominated diphenyl ethers; Wastewater; Electronic waste materials; Electric waste materials; Environmental; Polybrominated biphenyls; Tetrabromobisphenol A; Aryl phosphates; Polymeric materials;

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Determination of total phthalates in urine by isotope-dilution liquid chromatography-tandem mass spectrometry

Kato, K., Silva, M.J., Needham, L.L., Calafat, A.M.(*)

Div. Lab. Sci., Natl. Cent. Environ. Health, Cent. Dis. Control Prevention, Atlanta, GA 30341, USA

REF: J. Chromatogr. B 814(2) 2005 355-360

MS: Finnigan TSQ 7000, ESP, neg., CAD, SRM.

Keywords: Electrospray/MS/MS, phthalates; CAD; Urine; Isotope dilution; Phthalate metabolites; Hydrolysis;

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Analysis of tetracyclines in honey by high-performance liquid chromatography/tandem mass spectrometry

Khong, S.-P., Hammel, Y.-A., Guy, P.A.(*)

Nestle Res. Cent., Nestec Ltd., Vers-Chez-Les-Blanc, 1000 Lausanne 26, Switzerland

REF: Rapid Commun. Mass Spectrom. 19(4) 2005 493-502

MS: Finnigan TSQ Quantum Discovery, ESP, pos., CAD, SRM.

Keywords: Electrospray/MS/MS, antibiotics; CAD; Tetracyclines; Honey; Food; Tetracycline; Oxytetracycline; Doxycycline; Chlortetracycline;

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Urinary metabolites of di-n-octyl phthalate in rats

Silva, M.J.(*1), Kato, K.(1), Gray, E.L.(2), Wolf, C.(2), Needham, L.L.(1), Calafat, A.M.(1)

(1) Div. Lab. Sci., Natl. Cent. Environ. Health, Cent. Dis. Control Prevention, Mailstop F17, 4770 Buford Hwy NE, Atlanta, GA 30341, (2) Reproductive Toxicol. Div., Endocrinol. Branch, Natl. Health Environ. Effects Res. Lab., US EPA, Research Triangle Park, NC 27705, USA

REF: Toxicology 210(2/3) 2005 123-133

MS: Finnigan TSQ Quantum, ESP, pos., CAD, SRM.

Keywords: Electrospray/MS/MS, phthalates; CAD; Dioctyl phthalate, metabolism; Phthalic acid; Urine; Plasticizers;

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This bibliography was prepared for Thermo Electron Corporation by HD Science Ltd.

last updated 6-JUL-2005